Course Syllabus

Course Information：

Year-Semester Course Number Course Name Phase Credits Hours Required/Elective Instructor Class Student NO. Withdraw Note

Fall Semester
Year 2018 246882 Advances in Instrumental Analysis 1 3.0 3 ★ SHENG-MING CHEN IDEOM 13 0 chemical building 207 room

Year-Semester	Course Number	Course Name	Phase	Credits	Hours	Required/Elective	Instructor	Class	Student NO.	Withdraw	Note
Fall Semester Year 2018	246882	Advances in Instrumental Analysis	1	3.0	3	★	SHENG-MING CHEN	IDEOM	13	0	chemical building 207 room

Course Plan：

Instructor SHENG-MING CHEN

Email smchen@ntut.edu.tw

Last Updated 2018-06-04 20:28:48

Course Objective 課程兩個主要目標為光譜學方法及分離方法。光譜學方法內容含紫外、可見、紅光、核磁、x-ray等光譜法。電子譜及質譜也將被討論。分離方法方面有液層、氣層、膠層等層析法。分離後串聯之光譜分析也會學習。 This course is designed to provide graduate students an advanced, cohesive understanding of advanced instruments, analytical chemistry methods and instrumentation principles, theory to promote success in their graduate careers. Core concepts will be presented by both students and course instructor via lecture presentations, discussions and with real time experiments. The curriculum will be wide in scope incorporating aspects of trouble shooting, experimental result discussion, chemical measurements, modern analytical instrumentation, and determination of chemical structure via analytical techniques. Special emphasis will be put on the appropriate preparation, and meaningful presentation, of scientific results. The student is expected to dedicate significant effort both in and out of lectures to be successful.

Course Schedule Raman spectroscopy - Raman scattering - stoke's and anti stokes lines - instrumentation - differences between IR and Raman spectroscopy - mutual exclusion principle - applications - structural diagnosis. UV- Visible spectroscopy - Absorbtion laws - calculations involving Beer - lambert's law - instrumentation - spectrophotometer - block diagrams with description of components - theory - factors governing absorbtion maximum and intensity Infrared spectroscopy - principle - types of stretching and bending vibrations - vibrational frequencies - instrumentation - block diagram - source - detector and recorders Chromatography techniques -Principles adsorption, thin layer, partition and paper. chromatography column chromatography - and applications. Ion exchange chromatography - principle - resins - action of resins - experimental techniques - applications - Gas chromatography and high pressure liquid chromatogrphy - principles - experimental techniques - instrumentation and applications. AFM and STM - Principles, instrumentation, and applications in detailed study SEM and TEM: Principle and applications of compound, Different parts of compound microscope, resolving power, magnification power, numerical aperture and working distance. XPS- Principles, instrumentation, and applications in detailed study ATR and XRD - Principles, instrumentation, and applications in detailed study Mass spectroscopy, NMR- Principles, instrumentation, and applications in detailed study CV and SECM- Principles, instrumentation, and applications in detailed study

Evaluation and grading policy Group discussions: --------------------15% Exams (including final):-------------- 15% Class Presentations: -------------------15% Written Reports:------------------------ 25% Experimental results:-------------------20% In Class Participation:----------------- 10%

Materials All right reserved. Do not reproduce without permission.

Foreign-language textbooks:Yes
　

The access to curricular consultation

Note
　

Instructor	SHENG-MING CHEN
Email	smchen@ntut.edu.tw
Last Updated	2018-06-04 20:28:48
Course Objective	課程兩個主要目標為光譜學方法及分離方法。光譜學方法內容含紫外、可見、紅光、核磁、x-ray等光譜法。電子譜及質譜也將被討論。分離方法方面有液層、氣層、膠層等層析法。分離後串聯之光譜分析也會學習。 This course is designed to provide graduate students an advanced, cohesive understanding of advanced instruments, analytical chemistry methods and instrumentation principles, theory to promote success in their graduate careers. Core concepts will be presented by both students and course instructor via lecture presentations, discussions and with real time experiments. The curriculum will be wide in scope incorporating aspects of trouble shooting, experimental result discussion, chemical measurements, modern analytical instrumentation, and determination of chemical structure via analytical techniques. Special emphasis will be put on the appropriate preparation, and meaningful presentation, of scientific results. The student is expected to dedicate significant effort both in and out of lectures to be successful.
Course Schedule	Raman spectroscopy - Raman scattering - stoke's and anti stokes lines - instrumentation - differences between IR and Raman spectroscopy - mutual exclusion principle - applications - structural diagnosis. UV- Visible spectroscopy - Absorbtion laws - calculations involving Beer - lambert's law - instrumentation - spectrophotometer - block diagrams with description of components - theory - factors governing absorbtion maximum and intensity Infrared spectroscopy - principle - types of stretching and bending vibrations - vibrational frequencies - instrumentation - block diagram - source - detector and recorders Chromatography techniques -Principles adsorption, thin layer, partition and paper. chromatography column chromatography - and applications. Ion exchange chromatography - principle - resins - action of resins - experimental techniques - applications - Gas chromatography and high pressure liquid chromatogrphy - principles - experimental techniques - instrumentation and applications. AFM and STM - Principles, instrumentation, and applications in detailed study SEM and TEM: Principle and applications of compound, Different parts of compound microscope, resolving power, magnification power, numerical aperture and working distance. XPS- Principles, instrumentation, and applications in detailed study ATR and XRD - Principles, instrumentation, and applications in detailed study Mass spectroscopy, NMR- Principles, instrumentation, and applications in detailed study CV and SECM- Principles, instrumentation, and applications in detailed study
Evaluation and grading policy	Group discussions: --------------------15% Exams (including final):-------------- 15% Class Presentations: -------------------15% Written Reports:------------------------ 25% Experimental results:-------------------20% In Class Participation:----------------- 10%
Materials	All right reserved. Do not reproduce without permission. Foreign-language textbooks:Yes
The access to curricular consultation
Note